Applications

Some of the notes appearing on this page can be downloaded in .pdf format by clicking on the note number. PDF files can be read and printed using Adobe Acrobat Reader, which you can download for free. If the notes you would like are not available for download, please contact us and we will send them to you.

Technical Notes:
FTIR Basics

Application Notes: Please click on your area(s) of interest.
Gas Phase Analysis
General Spectroscopy
Laboratory
Open Path Analysis
Petroleum Analysis
Semiconductors
Software and Methods


New or Special Items: Several new items are now available:

  1. TN-102
    "Making Your Own Reference Spectra, Method, and Determining Cell Pathlength Using AutoQuant 3.x"
  2. AP-156
    "The MIDAC Low Moisture in Corrosive Gases Process Analyzer for Continuous On-Line Process Analysis."
  3. AP-157
    "Validation Study Of FTIR-Based Emissions Measurements At A Municipal Waste Combustor "
  4. NIOSH Method 3800 - Organic and Inorganic gases by Extractive FTIR Spectrometry : This comprehensive document describing the NIOSH method for gas phase FTIR analysis is available from the NIOSH website. Follow the link to the NIOSH website and search for Method 3800 to access the document.


FTIR Basics

TN-100

Fundamental Infrared Spectroscopy. H. Phan

TN-101 FTIR Sampling Techniques. H. Phan

TN-102

Making Your Own Reference Spectra, Method, and Determining Cell
Pathlength Using AutoQuant 3.x.
P Zemek, Ph.D.

| Top | Contact Us |

Gas Phase Analysis 

AP-118

Extractive FTIR: Manufacturing Process Optimization Study. J.S. Eldridge, J.W. Stock, W.K. Reagen and J.M. Osborne, 3M Environmental Technology & Services, St. Paul, MN, (Air & Waste Management Assn.).

AP-119

Comprehensive VOC Source Emissions Assessment. A Combined Approach of EPA Method TO-14, EPA Method TO-11, and Extractive FTIR. W.K. Reagen, Margaret M. DePuydt and Brian D. Wright, 3M Environmental Technology & Services, St. Paul, MN, (Air & Waste Management Assn.).

AP-121

Passive Fourier Transform Infrared (FT-IR) Monitoring of SO2 in Smokestack Plumes: A Comparison of Remote Passive Spectra of an Actual Hot Plume with Emission Spectra of an Actual Hot Plume with Emission Spectra Collected with a Heatable Cell. C.T. Chaffin, T.L. Marshall, AeroSurvey, Inc., Manhatten, KS. R.J. Combs, R.B. Knapp, U.S. Army Edgewood Research, Development and Engineering Center, Aberdeen Proving Ground, MD. R.T. Kroutil, W.G. Fateley, R.M. Hammaker, Kansas State University, Manhatten, KS. (Optical Sensing for Environmental and Process Monitoring, November 1994).

AP-122

Protocol for the use of Extractive Fourier Transform Infrared (FTIR) Spectrometry for the Analyses of Gaseous Emissions from Stationary Sources. From the Environmental Protection Agency (EPA) technology transfer network (TTN).

AP-123

FTIR Monitoring for Real Time Organic Emissions Measurement and Process Control at Military or Industrial Coating Facilities and Other Solvent Operations. Jacqueline Ayer, Air Quality Specialists, Newport Beach, CA. Glen M. Williams, Infrared Analysis, Anaheim, CA.(Air & Waste Management Association, June 1996).

AP-124

Analysis of Volatile Organic Compounds (VOCs) by Extractive FTIR Spectroscopy. Duane E. Bartak, Russell A. Wiley, Christopher Crome, Marjorie Rover, University of Northern Iowa, Cedar Falls, IA. (Air & Waste Management Association, June 1996).

AP-126

Production Facility Emissions Assessment Using Heated Extractive FTIR Spectroscopy and EPA Method 25A. William K. Reagan, 3M Environmental Laboratory, St. Paul, MN. Brian D. Wright, MIDAC Corporation, Irvine, CA. (Air & Waste Management Association, June 1996).

AP-131

Quantitative Measurements by Fourier-Transform Infrared Spectroscopy of Toxic Gas Production During Inhibition of JP-8 Fires by CF3Br and C3F7H. Steven H. Modiano, Kevin L. McNesby, Paul E. Marsh, William Bolt, And Craig Herud (Applied Optics, pages 4004-4008, July 20, 1996).

AP-139

EPA Test Method 320: Measurement of Vapor Phase Organic and Inorganic Emissions by Extractive Fourier Transform Infrared (FTIR) Spectroscopy.

AP-147 Fourier Transform Infrared Method Validation at a Carbon Bed Solvent Unit for Four Gaseous Hydrocarbons, W. K. Reagen, B. D. Wright, D. J. Krueger, G. M. Plummer (Environ. Sci. Technol., 1999, 33,10,1752).
AP-156 The MIDAC Low Moisture in Corrosive Gases Process Analyzer for Continuous
On-Line Process Analysis.
P.G. Zemek

| Top | Contact Us |

General Spectroscopy

AP-101

Infrared Spectroscopic Analysis of HCl and DCl. H. Phan

AP-147 Fourier Transform Infrared Method Validation at a Carbon Bed Solvent Unit for Four Gaseous Hydrocarbons, W. K. Reagen, B. D. Wright, D. J. Krueger, G. M. Plummer (Environ. SCI Technol., 1999, 33,10,1752).

| Top | Contact Us |

Laboratory

AP-103

Quantitative Analysis of Epoxy Mixing Ratios Using Partial Least Squares Analysis of FTIR Spectra. W. Britton

AP-104

Compact FTIR Spectrometer Inside A Glovebox: IR Spectroelectrochemistry and other Applications. A. Saravanamuthu, A. Bruce, M. Bruce

AP-105

Detection of Extractable Hydrocarbons in Flourocarbon-113 Using FTIR Spectrometry. H. Phan

AP-106

Detection of Extractable Hydrocarbons Using an FTIR Spectrometer with an InSb Detector. H. Phan

AP-108

Analysis of Polymers Using Attenuated Total Reflectance FTIR Spectroscopy. H. Phan

AP-117

On-Site Fourier Transform-Infrared Spectrometry at an Archaeological Excavation. Stephen Weiner, Paul Goldberg (Spectroscopy, February 1990).

| Top | Contact Us |

Open Path Analysis

AP-107

Measurements of Chemical Emissions Using FTIR Spectroscopy. H. Phan, G. Auth (American Laboratory News, August 1993).

AP-110

Development of Sampling Strategies for Open Path FTIR Monitoring of Fugitive Emissions. C. Chaffin

AP-111

Analyzing Air from a Single Beam Spectrum. P.Hanst (Spectroscopy Magazine, November, 1993).

AP-112

Detection of Fugitive Emissions Using Passive Remote FTIR Spectroscopy. J. Demirgian

AP-113

Real-time Data Collection Programs for a Commercial Passive FT-IR Remote Sensor. R. Kroutil, M. Housky, G.W. Small (Spectroscopy, February 1994).

AP-114

Distinguishing Benzene's 674cm-1 Absorption Band from Interferences in Open-Path FTIR Spectra. C. Chaffin, T. Marshall (American Environmental Laboratory, April, 1995).

AP-115

An Introduction to Open-Path FTIR Atmospheric Monitoring. TL Marshall, CT Chaffin, R.M. Hammaker, W.G. Fateley.

AP-116

FTIR and Fugitive Emissions. TL Marshall, CT Chaffin, M.D. Tucker, W.G. Fateley (Environmental Testing and Analysis, May 1994).

AP-120

Infrared Analysis of Volcanic Plumes: A Case Study in The Application of Open-Path FT-IR Monitoring Techniques. Charles T. Chaffin, TL Marshall, W.G. Fateley and R.M. Hammaker, (Spectroscopy Europe, May/June 1995).

AP-128

Accuracy and Advantages of Synthetic Calibration of Smoke Spectra. Robert J. Yokelson, University of Montana, David W.T. Griffith, University of Wollongong-Australia, James B. Burkholder, University of Colorado, Darold E. Ward, USDA Forest Service Intermountain Research Station. (Proceedings of the Air and Waste Management Association Symposium on Optical Remote Sensing for Environmental and Process Monitoring, San Francisco, Sept. 25-27, 1995).

AP-129

Open-path Fourier Transform Infrared Studies of Large-scale Laboratory Biomass Fires. Robert J. Yokelson, David W. T. Griffith, Darold E. Ward (Journal of Geophysical research, Vol. 101, No. D15, pages 21,067-21,080, September 20, 1996).

AP-130

Emissions From Smoldering Combustion of Biomass Measured by Open-path FTIR. Robert J. Yokelson, University of Montana, Ronald Susott, Darold E. Ward, James Reardon, USDA Forest Service, David W. T. Griffith, University of Wollongong-Australia.

AP-133

Optical Measurement of Toxic Gases Produced During Firefighting Using Halons. Kevin L. McNesby, Robert G. Daniel, Andrzej W. Miziolek, and Steven H. Modiano.

AP-134

Effect of Ambient Blackbody and Other IR Emission Sources on Bistatic, Open-Path FTIR Measurements. Edgar Thompson, Jr., Jeffrey Childers and George Russwurm, ManTech Environmental Technology, Inc., Research Triangle Park, NC (AWMA, San Antonio, June 1995)

AP-144 Thermal Stability Evaluation for Passive FTIR Spectrometry. R. J. Combs (Field Analytical Chemistry and Technology, 3, 2, 81).
AP-145 Signal Processing Strategies for Passive FT-IR Sensors, R. E. Shaffer, R. J. Combs (SPIE Conference on Electro-Optical Technology for Remote Chemical Detection and Identification III, 3383, April 1998).
AP-150 Effect of Spectral Resolution on Pattern Recognition Analysis Using Passive Fourier Transform Infrared Sensor Data, A. S. Bangalore, J. C. Demirgian, A. S. Boparai, G. W. Small (Applied Spectroscopy, 53, 11, 1382).
AP-151 Radiometric Linearity in Passive FTIR Spectrometry, R. T. Kroutil, R. J. Combs, R. B. Knapp (SPIE Conference on Internal Standardization and Calibration Architectures for Chemical Sensors, 3856,September 1999). 
AP-152 Emissions of formaldehyde, acetic acid, methanol, and other trace gases from biomass fires in Northa Carolina measured by airborne Fourier transform infrared spectroscopy, R. J. Yokelson, J. G. Goode, D. E. Ward, R. A. Susott, R. E. Babbitt, D. D. Wade, I. Bertschi, D. W. T. Griffith, W. M. Hao (J. of Geophys, Res., 1999, 104, D23, 30, 109).
AP-153 Trace gas emission from laboratory biomass fires measured by open-path Fourier transform infrared spectroscopy:  Fires in grass and surface fuels, J. G. Goode, R. J. Yokelson (J. of Geophys. Res,. 1999, 104, D17, 21, 237).
AP-154 Quantitative Analysis of Sulfur Dioxide with Passive Fourier Transform Infrared Remote Sensing Interferogram Data, M.J. Mattu, G.W. Small, R.J. Combs, R.B. Knapp, R.T. Kroutil (Applied Spectroscopy, 54, 3, 341).
AP-155 FT-IR Spectrometers Perform Environmental Monitoring, George M. Russwurm, Jeffrey W. Childers (Laser Focus World, April 1995)

| Top | Contact Us |

Petroleum Analysis

AP-109

FTIR Analysis of Oxygenates for Motor Gasoline. H. Phan

AP-127

Comprehensive Analysis of Reformulated Gasoline and Diesel Fuel Using Portable FTIR Instruments. Leslie M. Tack, Jennifer E. Lyons and Caroline M. Taylor, MIDAC Corporation.

AP-136

Determination of Weight Percent Oxygen in Commercial Gasoline: A Comparison Between FT-RAMAN, FT-IR, and Dispersive Near-IR Spectroscopies. John Cooper, Kent Wise, William Welch, Roy Bledsoe, and Michael Sumner (Applied Spectroscopy, Vol. 50, No. 7, July 1996)

AP-143  On the Prowl for Quality Gasoline, A. Merrick (R & D Magazine, October 1998).
AP-148 Standard Practice for Condition Monitoring of Used Lubricants by Trend Analysis Using Fourier Transform Infrared (FT-IR) Spectrometry (ASTM Draft).
AP-149 The MIDAC FOx FTIR Oil Analyzer for Laboratory, Field, Mobile, and On-line Applications, L. Tack (International Oil Analysis Exhibition, Tulsa, Oklahoma, October 1999).

| Top | Contact Us |

Semiconductors

AP-132

A Better Way to Clean CVD Chambers of Residual Oxides - Using FTIR Analysis, Scientists at 3M have shown that C3F8 produces less net PFC and CO2-Equivalent Emissions than C2F6. Vic Comello (R&D Magazine, pages 31-32, July 1997).

AP-135

Reducing PFC Emissions Using C3F8 - Based PECVD Clean. Sey-Ping Sun, David Bennett, Larry Zazzera, William Reagen (Semiconductor International, February 1998)

AP-137

Continuous In-Line Monitoring of Cl2 and HCl in Water-Vapor-Saturated Gas Streams Using Mass Spectrometry. Dr. Josep Arno (Spectroscopy, Vol. 13, No. 2, February 1998)

AP-138

Protocol For FTIR Measurements Of Fluorinated Compounds In Semiconductor Process Tool Exhaust. Dr. William Reagen (Sematech, 1997)

AP-140 Infrared Study of Process Emissions During C3F8/O2 Plasma Cleaning of Plasma Enhanced Chemical Vapor Deposition Chambers, L. Zazzera, W. Reagan, A. Cheng (Journal of the Electrochemical Society, 144, 10 3597).
AP-141   Application of FTIR for Monitoring Cleanroom Air and Process Emissions, L. Zazzera, W. Reagan (Solid State Technology Supplement, May 1998).
AP-142 Trace Water Vapor Determination in Nitrogen and Corrosive Gases Using Infrared Spectroscopy, L. H. Espinoza, T. M. Niemczyk, B. R. Stallard, M.J. Garcia (Sandia Report, SAND97-1494, UC-411, June 1997).

| Top | Contact Us |

Software and Methods

AP-100

FTIR Partial Least Squares Analysis of Cyclohexane Mixtures. W. Britton

AP-102

Computer Searching of FTIR Spectra. H. Phan

AP-125

An Examination of a Least Squares Fit FTIR Spectral Analysis Method. Grant M. Plummer, Rho Squared, Durham, NC. William K. Reagan, Minnesota Mining and Manufacturing (3M) Company, St. Paul, Minnesota. (Air & Waste Management Association, June 1996).

AP-128

Accuracy and Advantages of Synthetic Calibration of Smoke Spectra. Robert J. Yokelson, University of Montana, David W.T. Griffith, University of Wollongong-Australia, James B. Burkholder, University of Colorado, Darold E. Ward, USDA Forest Service Intermountain Research Station. (Proceedings of the Air and Waste Management Association Symposium on Optical Remote Sensing for Environmental and Process Monitoring, San Francisco, Sept. 25-27, 1995).

AP-146 Diagnostic Computer Program for FT-IR Spectrometry, R. T. Kroutil, R. J. Combs, R. B. Knapp (SPIE Conference on Online Chemical Process Monitoring with Advanced Techniques, 3537, November 1998).
AP-150 Effect of Spectral Resolution on Pattern Recognition Analysis Using Passive Fourier Transform Infrared Sensor Data, A. S. Bangalore, J. C. Demirgian, A. S. Boparai, G. W. Small (Applied Spectroscopy, 53, 11, 1382).

| Top | Contact Us |

 

| Products | Software | Sales Reps | Applications | OEM | Events | Corp. Profile | Home |